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We provide a seminal example of the utility of the 1,2-azaborine motif as a 4C+1N+1B synthon in organic synthesis. Specifically, conditions for practically scalable 1,2-azaborine photoisomerization in a flow reactor are reported to furnish aminoborylated cyclobutane derivatives. C-B bond functionalizations to furnish a diverse set of highly substituted cyclobutanes were also achieved.
This article was published in the following journal.
Name: Angewandte Chemie (International ed. in English)
Bacteriophytochromes are photoreceptors that regulate various physiological processes induced by photoisomerization in a linear tetrapyrrole chromophore upon red/far-red light absorption. Here, we inv...
Arylated cyclobutanes were accessed by a versatile palladium-catalyzed secondary C(sp3)-H activations exploiting chelation assistance by modular triazoles. The C-H arylation led to cyclobutane natural...
A new family of light driven molecular rotary motors, which can be synthesized from easily available precursor compounds and which are capable of completing a full 360° revolution by two photoisomeri...
cis,trans-1,2-Dideuterio-1,4-diphenyl-1,3-butadiene (ct-DPBd2) was synthesized and its cis-trans photoisomerization in cyclohexane-d12 (C6D12) at room temperature was monitored by 1H NMR spectroscopy....
Azoheteroarene photoswitches have attracted attention due to their unique properties. We present here the stationary photochromism and the ultrafast photoisomerization mechanism of thiophenylazobenzen...
Aim of the study is to evaluate adequacy of pain treatment in oncologic patients, accessing to our Radiotherapy Unit
Study personnel will use evidence based behavioral skills training procedures to coach educators to implement modules designed to increase the quality of educational services and access to...
The investigators will enroll a cohort of HIV-infected pregnant women accessing PMTCT services, to better understand the incremental benefits (e.g. reduction in HIV transmission, improvem...
Social insecurity is a significant cost in human terms (health and societal), it defines evil and can be identified as difficulties accessing health and especially water. We chose to take...
The mission of corrections is to provide custody, control and care for incarcerated individuals. United States prisons are required by constitutional law to provide adequate care for growi...
Four carbon cycloparaffin cyclobutane (the structural formula (CH2)4) and its derivatives.
Hand-sized cards with built-in computer chips used for accessing, storing, and protecting patients' medical information.
AMINO ACIDS composed of GLYCINE substituted at the nitrogen rather than the usual carbon position, resulting in the loss of HYDROGEN BONDING donors. Polymers of these compounds are called PEPTOIDS.
A class of enzymes that transfers substituted phosphate groups. EC 2.7.8.
Access to specialized care for transgender populations. Health systems organized to take account of the special healthcare needs of marginalized groups who may face barriers in accessing health services. (http://www.who.int/reproductivehealth/topics/linkages/guidance_package.pdf)